COMPACT PREPARATIVE SYSTEM (50 ml/min, TOY18DAD800)

4 channel Scanning 200-800 50ml/min 30MPa

Highly effective compact preparative system containing a UV-VIS DAD detector, a preparative gradient pump, an automatic inject valve and a fraction collector. The detector allows absorbance measuring at four wavelengths at the same time or scanning through entire spectrum.

Availability
Manufacturer
ECOM spol. s r.o.
Part number
ECS58P0X

The system is controlled by a built-in PC and touchscreen.

A modular solution allows configuring the unit according to customer needs. This system contains a detector with a wavelength range of 200 –  800 nm, a pump with flow rate up to 50 ml/min and fraction collector.

Main parts

TOY18DAD800L DETECTOR
It is a UV-VIS diode array detector, which allows measuring the absorbance of four wavelengths in a range of 200–800 nm simultaneously in one cell just as scanning of whole spectra. Standardly is assembled with preparative cell PLCC07L, but other cells are available.

ECF2096 FRACTION COLLECTOR
Fractions are collected according to chosen method, which is simply created using a touch screen. Racks for 8, 21,40 ml tubes, 60 ml vials or 12 funnels, 30 mm.

AUTOMATIC INJECT VALVE
The valve is driven by a step motor and it is automatically switched by software. The system also allows manual sample injection by opening the column.

SYSTEM PC INFO
Installed industrial PC with Intel Atom 4 core processor. OS Linux, Touch screen 12,1“ 1024 x 786, SW QUEEN controls: gradient, flow rate, wavelengths, fractions collection, etc. Remote administration is available. Possibility of measuring at four wavelengths at the same time or scanning through entire spectra. Furthermore, the possibility of displaying 3D data.
 

ECP2050 PREPARATIVE GRADIENT PUMP
Modified for the compact system, quaternary gradient pumps with flow rate up to 50 ml/min (30 MPa, 4351 PSI). Unit software includes a new learning algorithm for pulsation suppression and many testing and diagnostic functions.
 

COMPACT PREPARATIVE SYSTEM  
Interface 3xUSB, 2xLAN, RS232
Power supply 100 - 240 V AC
Power input 400 W
Dimensions W x H x D 500 x 678 x 482 mm (19.69 x 26.69 x 18.98")
Weight 55 kg (121.30 lb)
   
Detector  
Wavelength range  200 - 800 nm   (256 elements on CCD)
Number of channels (Signals) 4
Scan 200 - 800 nm,up to  20 Hz, step 1 nm
Typical spectral half-width 10 nm
Accuracy of adjustment / Reproducibility ± 1 nm / ±0.5 nm
Noise level at test cell (254 nm, TC 0.75s) ± 5 x 10-5 AU
Drift at test cell (254 nm after 1 h) 1 x 10-3 AU/hr
Materials in contact with mobile phase FEP; fused silica, stainless steel, PEEK
Time constant (T63) 0.5 s, 0.75 s, 1.0 s, 2.0 s, 4.0 s, 8.0 s, 16.0 s, 0.2 s, 0.1 s
   
Fraction collector  
 Available racks (two racks per unit) EC08 48 tubes of 8 ml
  EC21 36 tubes of 21 ml
 

EC40 24 tubes of 40 ml

  EC60 20 vials of 60 ml
  F12A 12 funnels, 30 mm

Maximum flow rate for tubes 8 ml

max. 50 ml/min
Maximum flow rate for tubes 21, 40 ml max. 300 ml/min
Maximum flow rate for vials 60 ml max. 300 ml/min
Maximum flow rate for funnels

max. 500 ml/min

Wetted materials  FEP, Tefzel®, PPS, KEL-F, PTFE, PEEK, SS 316, glass SIMAX
Input tubing OD 1/8“ x ID 1/16“ FEP
   
Pump  
Flow rate 0.1 – 50 ml/min
Maximum operating pressure 30 MPa (4351 PSI)
Flow rate setting  0.1 ml/min steps
Repeatability of flow rate adjusting ± 0.5 %
Accuracy of flow rate setting ± 2 %
Wetted materials stainless steel, PEEK, TefzelTM, PE, ceramic, seals *
   
Output capillary outer diameter 1/8”
Input tubing outer diameter 1/8”
Gradient valves control module - OPTIONALLY Up to six valves

 

 

 

Interface 3xUSB, 2xLAN, RS232
Power supply 100 - 240 V AC
Power input 490 W
Dimensions W x H x D 450 x 500 x 650 mm (17,72 x 19,69 x 25,59")
Weight 55 kg (21,30 lb)