COMPACT PREPARATIVE SYSTEMS

4 channel Scanning 200-800 10ml/min 50ml/min 250ml/min

A highly effective compact preparative system containing a UV-VIS DAD detector, a preparative gradient pump, an automatic inject valve, and a fraction collector. The detector allows absorbance measuring at four wavelengths at the same time and scanning through the entire spectrum.

Availability
Manufacturer
ECOM spol. s r.o.
Choose variant:
Image PN Name Flow rate [ml/min] Maximal pressure [MPa/PSI] UV-VIS detector range [nm] Sample loop [ml] Request quote
Image
ECS28 P Compact preparative system 250ml ; ECS28P0X
PN
ECS28P0X
Name
ECS28 P Compact preparative system 250 ml
Flow rate [ml/min]
0.5 – 250
Maximal pressure [MPa/PSI]
30 / 4351 up to 100 ml/min then linearly down up to 15 / 2176 at 250 ml/min
UV-VIS detector range [nm]
200 - 800
Sample loop [ml]
10
Actions
Image
ECS58 P Compact preparative system 50 ml,; ECS58P0X
PN
ECS58P0X
Name
ECS58 P Compact preparative system 50 ml
Flow rate [ml/min]
0.1 – 50
Maximal pressure [MPa/PSI]
30 / 4351
UV-VIS detector range [nm]
200 - 800
Sample loop [ml]
2
Actions
Image
ECS08 P Compact semi-preparative system 10 ml,  ECS08P0X
PN
ECS08P0X
Name
ECS08 P Compact semi-preparative system 10 ml
Flow rate [ml/min]
0.02 - 10.00
Maximal pressure [MPa/PSI]
40 / 5802
UV-VIS detector range [nm]
200 - 800
Sample loop [ml]
2
Actions

The system is controlled by a built-in PC and touch screen.

A modular solution allows configuring the unit according to customer needs. This system contains a detector with a wavelength range of 200–800 nm, a pump with a flow rate of up to 250; 50 and 10 ml/min according system type, and a fraction collector.

Main parts

TOY18DAD800L DETECTOR
It is a UV-VIS diode array detector, which allows measuring the absorbance of four wavelengths in a range of 200–800 nm simultaneously in one cell just as scanning of whole spectra. Standardly is assembled with preparative cell PLCC07L, but other cells are available.

ECF2096 FRACTION COLLECTOR
Fractions are collected according to the chosen method, which is simply created using a touch screen. Racks for 8, 21, 40 ml tubes, 60 ml vials, or 12 funnels, 30 mm.

AUTOMATIC INJECT VALVE
The valve is driven by a step motor and it is automatically switched by software. The system also allows manual sample injection by opening a column.

SYSTEM PC INFO
Installed industrial PC with Intel Atom 4 core processor. OS Linux, Touch screen 12,1“ 1024 x 786, SW QUEEN controls gradient, flow rate, wavelengths, fractions collection, etc. Remote administration is available. Possibility of measuring at four wavelengths at the same time and scanning through entire spectra. Furthermore, the possibility of displaying 3D data.
 

ECP PREPARATIVE GRADIENT PUMP
Modified for the compact system, quaternary gradient pump with flow rate according system type up to 250; 50 or 10 ml/min . Unit software includes a new learning algorithm for pulsation suppression and many testing and diagnostic functions.

 

COMPACT PREPARATIVE SYSTEM      
Interface 3xUSB, 2xLAN, RS232    
Power supply 100 - 240 V AC    
Power input 400 W    
Dimensions W x H x D 500 x 678 x 482 mm (19.69 x 26.69 x 18.98")    
Weight 55 kg (121.30 lb)    
       
Detector      
Wavelength range  200 - 800 nm   (256 elements on CCD)    
Number of channels (Signals) 4    
Scan 200 - 800 nm, up to  20 Hz, step 1 nm    
Typical spectral half-width 10 nm    
Accuracy of adjustment / Reproducibility ± 1 nm / ±0.5 nm    
Noise level at test cell (254 nm, TC 0.75s) ± 5 x 10-5 AU    
Drift at test cell (254 nm after 1 h) 1 x 10-3 AU/hr    
Materials in contact with the mobile phase FEP; fused silica, stainless steel, PEEK    
The time constant (T63) 0.5 s, 0.75 s, 1.0 s, 2.0 s, 4.0 s, 8.0 s, 16.0 s, 0.2 s, 0.1 s    
       
Fraction collector      
 Available racks (four racks per unit) EC08 48 tubes of 8 ml (OD 12 mm) (384 ml/rack)    
  EC21 36 tubes of 21 ml (OD 16 mm) (756 ml/rack)    
 

EC40 24 tubes of 40 ml (OD 20 mm) (960 ml/rack)

   
  EC60 20 vials of 60 ml (OD 27.5 mm) (1200 ml/rack)    
  F12A 12 funnels, 30 mm    

Maximum flow rate for tubes 8 ml

max. 50 ml/min    
Maximum flow rate for tubes 21, 40 ml max. 300 ml/min    
Maximum flow rate for vials  60 ml max. 300 ml/min    
Maximum flow rate for funnels max. 500 ml/min    

Wetted materials

FEP, Tefzel®, PPS, KEL-F, PTFE, PEEK, SS 316, glass SIMAX    
Input tubing OD 1/8“ x ID 1/16“ FEP    
       
Pump  For ECS28P0X For ECS58P0X  For ECS08P0X
Flow rate 0.5 – 250 ml/min 0.1 - 50 ml/min 0.02 - 10 ml/min
Maximum operating pressure 30 MPa (4351 PSI) up to 100 ml/min then  linearly down up to  30 MPa (4351 PSI) 40 MPa (5802 PSI)
15 MPa (2176 PSI) at 250 ml/min    
Flow rate setting  0.1 ml/min steps  0.1 ml/min steps 0.01  ml/min steps
Repeatability of flow rate adjusting ± 0,5 %  ± 0,5 % ± 0.5 %
Accuracy of flow rate setting ± 2 %  ± 2 % ± 2 %
Wetted materials stainless steel, PEEK, TefzelTM, PE, ceramic, seals   stainless steel, PEEK, TefzelTM, PE, ceramic, seals  stainless steel, PEEK, TefzelTM, PE, ceramic, seals 
       
Output capillary outer diameter 1/8”  1/16”  1/16” 
Input tubing outer diameter 3/16”   1/8”  1/8” 
       

 

 

Interface 3xUSB, 2xLAN, RS232
Power supply 100 - 240 V AC
Power input 490 W
Dimensions W x H x D 500 x 678 x 482 mm (17,72 x 19,69 x 25,59")
Weight 55 kg (121,30 lb)